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13C-NMR- Spektroskopie: Eine Einf?hrung by L. Ernst (German) Paperback Book
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Located in: Fairfield, Ohio, United States
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eBay item number:395152040740
Item specifics
- Condition
- ISBN-13
- 9783798505643
- Book Title
- 13C-NMR- Spektroskopie
- ISBN
- 9783798505643
- Series
- Universitätstaschenbücher Ser.
- Publication Year
- 1980
- Type
- Textbook
- Format
- Trade Paperback
- Language
- German
- Publication Name
- 13c-NMR- Spektroskopie : Eine Einführung
- Item Length
- 8in
- Publisher
- Steinkopff, Dietrich
- Item Width
- 5in
- Item Weight
- 16 Oz
- Number of Pages
- VIII, 124 Pages
About this product
Product Information
Die Anwendung physikalischer Methoden in der Chemie hat in den vergangenen J ahrzehnten einen lebhaften Aufschwung genommen. Insbesondere die spektroskopischen Techniken spielen heute bei der Untersuchung von MolekUleigenschaften eine hervorragende Rolle. Kein rationell arbeitender Chemiker, sei er praparativ tatig oder mit der Isolierung von Naturstoffen beschaftigt, kann es sich leisten, auf die Dienste dieser Techniken zu verzichten. Vor allem die Kernresonanz-Spektroskopie (NMR) ist zu einem aufierst wichtigen Hilfsmittel des Chemikers geworden. Seit dem Erscheinen des ersten kommerziellen NMR-Spektrometers (1952) bis zum Ende der Sechziger Jahre beschrankte sich der Anwen- dungsbereich der NMR-Spektroskopie aus Empfindlichkeitsgrunden in der organischen Chemie hauptsachlich auf IH-NMR-Spektren, in der anorganischen Chemie daruber hinaus auf "B_, 19F_ und 31p_ NMR-Spektren. Der urn das Jahr 1965 einsetzende technologische Fortschritt erlaubte die Entwicklung von leistungsfahigen IlC-NMR- Spektrometern, die seit 1969 auf dem Markt sind. Seitdem ist die 13C_ NMR-Spektroskopie zu einer bedeutenden analytischen Technik ge- worden und ist der IH-NMR-Spektroskopie zumindest ebenbUrtig. Sie wird inzwischen routinemaBig bei der StrukturaufkIarung unbekann- ter Molekule eingesetzt, und es erscheint daher wichtig, daB ein Che- miker schon wahrend seiner Ausbildung mit dieser Methode vertraut gemacht wird. Das vorliegende Taschenbuch solI auf elementarem Niveau eine Ein- fUhrung fUr den deutschsprachigen Studenten geben und ihn nach der Lekture in die Lage versetzen, die 13C-NMR-Spektroskopie bei seiner Arbeit praktisch zu nutzen. Zugleich sollen die hier vermittelten Grundlagen den Einstieg in die weiterfUhrende Literatur erleichtern. Eine gewisse Vertrautheit mit den Grundzugen der IH-NMR-Spektro- skopie (vgl. Au/tIDudek, Protonen-Kernresonanz-Spektroskopie, UTB 842) ware beim Studium des vorliegenden Buches vorteilhaft.
Product Identifiers
Publisher
Steinkopff, Dietrich
ISBN-10
3798505640
ISBN-13
9783798505643
eBay Product ID (ePID)
4999305
Product Key Features
Publication Name
13c-NMR- Spektroskopie : Eine Einführung
Format
Trade Paperback
Language
German
Series
Universitätstaschenbücher Ser.
Publication Year
1980
Type
Textbook
Number of Pages
VIII, 124 Pages
Dimensions
Item Length
8in
Item Width
5in
Item Weight
16 Oz
Additional Product Features
Series Volume Number
1061
Number of Volumes
1 Vol.
Lc Classification Number
Qd71-142
Table of Content
1. Kernmagnetische Resonanz.- 1.1. Magnetische Eigenschaften von Atomkernen.- 1.2. Verhalten von Atomkernen im Magnetfeld.- 1.3. Die Resonanzbedingung.- 1.4. Die spektralen Parameter.- 1.5. Das Empfindlichkeitsproblem in der 13C-NMR-Spektroskopie.- 2. Puls-Fourier-Transformations-Technik.- 2.1. Das Puls-Experiment.- 2.2. Fourier-Transformation.- 2.3. Mathematische Manipulation des FID.- 2.4. Genauigkeit der spektralen Parameter.- 3. Chemische Verschiebungen von 13C-Kernen.- 3.1. Additivität von Verschiebungsinkrementen.- 3.2. Einflüsse von Substituenten auf chemische Verschiebungen.- 3.3. Chemische Verschiebungen wichtiger Substanzklassen.- 4. Spin-Kopplungen mit 13C-Kernen.- 4.1. Kopplungen zwischen 13C und 1H.- 4.2. Kopplungen zwischen 13C und 13C.- 4.3. Kopplungen zwischen 13C und Heterokernen.- 5. Signalzuordnungstechniken in der13C-NMR-Spektroskopie.- 5.1. Interpretation von chemischen Verschiebungen und Kopplungskonstanten.- 5.2. Doppelresonanz-Methoden.- 5.3. Isotopenmarkierung.- 5.4. Anwendung paramagnetischer Verschiebungsreagenzien.- 5.5. Spin-Gitter-Relaxation.- 6. Einige Beispiele zur Strukturaufklärung.- 6.1. Ein Hexahydro-oxo-thienopyridin.- 6.2. 3'-Amino-3'-desoxy-adenosin-2'-thionphosphorsäure-2':3'-cycloamid.- 6.3. Emmotin-A.- 7. Anhang.- 7.1. Lösungen der Übungsaufgaben.- 7.2. Ausgewählte Literatur.- 7.3. Eigenschaften wichtiger Lösungsmittel.
Copyright Date
1980
Topic
Chemistry / Analytic
Lccn
81-126833
Intended Audience
Scholarly & Professional
Illustrated
Yes
Genre
Science
Item description from the seller
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Premier Books LLC
David Taylor
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